The University of North Carolina
at Pembroke
Department of Chemistry and Physics
Course: CHM 2510-001, "Organic Chemistry II"
Lab: CHM 2510-700 "Organic Chemistry II Lab"
Term: Fall 2009
Meetings for the course: TR 12:30 pm – 1:45 pm, SCI
3202
Meetings for the Lab: T 2:00 pm – 4:45 pm, SCI
3115
Office Hours: 8:00 am-9:00 am T, 9:00
am-10:00 am WF 2:00
pm-3:00 pm MR or by appointment
Professor: Cornelia Tirla
Literature Resources:
class text –K.P.C. Vollhardt, N.E. Schore "Organic
Chemistry" fifth edition, Freeman
Lab text –
K. Williamsom, R.D. Minard, K.M. Masters ÒMacroscale and Microscale Organic ExperimentsÓ, fifth edition.
web literature - some
useful resources are:
Objectives: The activities associated with this course are designed to provide
students an understanding of the fundamental principles of organic chemistry
and to foster the ability to solve problems, to write and speak clearly, and to
think critically and creatively.
Description: This course will be concerned
with the knowledge and understanding of the fundamental theories and practices
of organic chemistry sufficient for subsequent entry into programs/courses
requiring an organic chemistry competency, the workforce, or graduate
professional programs of study. Emphasis will be placed on classification of
compounds, names and structures, reactions, synthesis and mechanism;
introductory spectroscopy and bio-organic topics.
Lab safety: Students must follow all written and verbal instructions regarding
safe lab procedures. A written copy of lab safety policies will be provided.
Failure to comply with these rules may result in dismissal from the lab. Eye
protection must be worn at all times in the lab. Personal electronic devices
such as cell phones and pagers should not be brought to the lab with you.
Format: The conventional lecture format
will be the primary teaching method employed in this course. Because of
the importance of the literature data in chemistry, students should bring
the class text book to each class meeting to allow
for participation in group problem-solving sessions.
Lab will begin with a briefing in a
classroom to be designated by the instructor.
Please read your lab and be prepared with any questions you have regarding the
procedure or the written report. During the lab period please concentrate first
on completing the required experimental procedures, measurements, and
observations. Calculations and questions are a secondary priority if they can
be done outside the lab period. These priorities are essential if labs are to
be completed. Information for each experiment must be recorded in the lab
notebook and initialed by the instructor prior to leaving lab. Reports to turn
in will be written from the information recorded in the lab notebook. The
format for notebooks and written reports will be provided for each experiment.
Because of the importance of the safety in chemistry, students should bring lab coat and appropriate safety
eyewear. All the experiments will be
described in a quad ruler bound notebook (available from the
instructor).
NOTE:
Any student with a documented disability needing academic adjustments is
requested to speak directly to Disability Support Services and the instructor,
as early in the semester (preferably within the first week) as possible.
All discussions will remain confidential.
Evaluation/Grading: Graded assignments will be scored on a 100-point scale. Letter grades
for the course will be assigned according to the following scale:
100-95=A, 94-90=A-, 89-87=B+, 86-83=B, 82-80=B-, 79-77=C+, 76-73=C, 72-70=C-,
69-67=D+, 66-63=D, 62-60=D-, 59 and below=F. These letter grades will
then be converted to the 4-point QPA scale by the University Registrar's Office
prior to being recorded on student transcripts (see p. 42 of the UNCP catalog).
Class(75%): Graded assignments
for this course will include four preterm tests (60%) and a comprehensive final
exam (15%). Pertinent questions
and problems will frequently be suggested for work outside of class, though
submission of these assignments is not required.
Lab (25%) : Graded assignments for
this course will include the lab reports (60%), notebook (10%) a midterm test
(15%) and a final exam (15%). All
lab reports are due the next week following the experiment. For each day of delay you lose 10% of the grade.
Now lab report will be do after 10 days. Pertinent questions and problems
will frequently be suggested for work outside of class, though submission of
these assignments is not required.
Attendance: Poor attendance typically results in
poor performance on graded assignments and, consequently, low course
grades. Though attendance per se is not factored into this
course's grading scheme, students will be required to sign an attendance roster
at each class meeting for purely bookkeeping purposes. Attendance at all scheduled lab sessions is required.
There will be no make up labs. If absence is unavoidable excuses must be
written and submitted one week prior to or following the absence. Additional
documentation may be required. Unavoidable absences are considered for personal
or immediate family illness, death in the immediate family, or business
commitments that are verified by your employer in writing. Missed labs that do
not meet the above criteria will result in a grade of Ò0Ó. No student will
receive credit for the lab if he or she misses in excess of two lab periods.
Honor Code:
Students are expected to follow the UNCP Honor Code (see pp. 51-53 of the
UNCP catalog); settled cases involving first-offense
violation of the Honor Code will result in a minimum penalty of course failure.
Notes or book are not allowed during the test. Only material provided by the
instructor can be used during the test.
|
Dates
four the class |
Chapters |
Topics |
||||||
|
|
Tuesday |
Thursday |
|
|
||||
|
|
|
August 20 |
|
Review. |
||||
|
|
August 25 |
August 27 |
Ch 11 |
Alkenes.IR Spectroscopy
|
||||
|
|
September 1 |
September 3 |
Ch 12 |
Reactions of Alkenes. |
||||
|
|
September 8 |
September 10 |
Ch 13 |
Alkynes |
||||
|
|
September 15 |
September 17 |
Ch 11-13 |
Review. Test 1 |
||||
|
|
September 22 |
September 24 |
Ch 14, 15 |
Delocalized Pi system. UV-Vis Spectroscopy. Benzene and Aromaticity |
||||
|
|
September 29 |
October 1 |
Ch 15,16 |
Benzene and Aromaticity Electrophilic attack
on benzene derivatives. |
||||
|
|
October 6 |
October 8 |
Ch 14-16 |
Review. Test 2 |
||||
|
|
October 13 |
Fall
break |
Ch 17 |
Aldehydes and Ketones |
||||
|
|
October 20 |
October 22 |
Ch 18 |
Enols and Enolates |
||||
|
|
October 27 |
October 29 |
Ch 17-18 |
Review. Test 3 |
||||
|
|
November 3 |
November 5 |
Ch 19, 20 |
Carboxylic acids, Carboxylic acids derivatives |
||||
|
|
November 10 |
November 12 |
Ch 20, 21 |
Carboxylic acids derivatives Amines derivatives |
||||
|
|
November 17 |
November 19 |
Ch 19 -21 |
Review. Test 4 |
||||
|
|
November 24 |
Holyday |
Ch 22 |
Benzene substituets |
||||
|
|
December 1 |
December 3 |
Ch 22, 24 |
Carbohydrates Amino acids, Peptides and Proteins. Final Review |
||||
|
December 8 |
Final
test |
All the Ch. |
||||||
|
Laboratory. Chapters.Topics
|
||
|
Tuesday |
|
|
|
August 25 |
|
Lab1. Introduction, Safety, Policies |
|
September 1 |
|
Lab 2. NMR , Discussion,
Examples |
|
September 8 |
|
Lab 3. IR Discussion/ Use, |
|
September 15 |
|
Lab 4. Dry
lab. Analysis of IR, NMR spectra |
|
September 22 |
|
Lab 5. Column Chromatography |
|
September 29 |
|
Lab 6. Bromination of
Cholesterol |
|
October 6 |
|
Lab 7. Nitration of methyl benzoate |
|
October 13 |
|
Lab 8. Midterm test |
|
October 20 |
|
Lab 9. Dibenzalacetone by the Aldol Condensation |
|
October 27 |
|
Lab 10. Synthesis of aspirin |
|
November 3 |
|
Lab 11. Acetanilide : Acetylation
in aqueous solution. |
|
November 10 |
|
Lab 12. Dyes. Orange II |
|
November 17 |
|
Lab 13. Dyes. Methyl Orange |
|
November 24 |
|
Lab 14. Review,
Check out. Final test. |